Handbook of analytical instruments
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| Main Author: | |
|---|---|
| Format: | Electronic eBook |
| Language: | English |
| Published: |
New York, N.Y. :
McGraw-Hill Education LLC.,
c2006.
|
| Edition: | 2nd edition. |
| Subjects: | |
| Online Access: | https://www.accessengineeringlibrary.com/content/book/9780070604605 |
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Table of Contents:
- A. Preface to the second edition
- B. Acknowledgements
- C. Preface to the first edition
- 1. Fundamentals of analytical instruments
- Elements of an analytical instrument
- Sensors and transducers
- Signal conditioning in analytical instruments
- Read-out (display) systems
- Intelligent analytical instrumentation systems
- Pc-based analytical instruments
- Performance requirements of analytical instruments
- Instrument calibration techniques
- Validation
- 2. Colorimeters and spectrophotometers (visible?ultraviolet)
- Electromagnetic radiation
- Laws relating to absorption of radiation
- Absorption instruments
- Ultraviolet and visible absorption spectroscopy (uv?vis)
- Colorimeters/photometers
- Spectrophotometers
- Sources of error in spectrophotometric measurements
- Calibration
- 3. Infrared spectrophotometers
- Infrared spectroscopy
- Basic components of infrared spectrophotometers
- Types of infrared spectrophotometers
- Sample handling techniques
- Fourier transform infrared spectroscopy (ftir)
- Calibration
- Attenuated total reflectance (atr) technique
- 4. Flame photometers
- Principle of flame photometry
- Constructional details of flame photometers
- Types of flame photometers
- Clinical flame photometers
- Accessories for flame photometer
- Expression of concentration
- Interferences in flame photometry
- Procedure for determinations
- 5. Atomic absorption spectrophotometers
- Atomic absorption spectroscopy
- Atomic absorption instrumentation
- Sources of interferences
- Meter scale
- 6. Fluorimeters and phosphorimeters
- Fluorescence spectroscopy
- Principle of fluorescence
- Measurement of fluorescence
- Spectrofluorimeters
- z#REF!Microprocessor-based spectrofluorometer
- Measurement of phosphorescence
- 7. Raman spectrometer
- The raman effect
- Raman spectrometer
- Pc-based raman spectrometer
- Infrared and raman microspectrometry
- 8. Photoacoustic and photothermal spectrometers
- Photoacoustic spectroscopy
- Photothermal spectroscopy
- 9. Mass spectrometer
- Basic mass spectrometer
- Principle of operation
- Types of mass spectrometers
- Components of a mass spectrometer
- Inductively coupled plasma?mass spectrometer
- Trapped ion mass analyzers
- Ion cyclotron resonance (icr) mass spectrometery
- Quadrupole ion trap mass spectrometer
- Resolution in mass spectrometry
- Applications of mass spectrometry
- Gas chromatograph?mass spectrometer (gc?ms)
- Liquid chromatograph?mass spectrometer
- Tandem mass spectrometry (ms/ms)
- 10. Nuclear magnetic resonance spectrometer
- Nuclear magnetic resonance spectroscopy
- Principle of nmr
- Types of nmr spectrometers
- Constructional details of nmr spectrometer
- Varian t-60a nmr spectrometer
- Sensitivity enhancement for analytical nmr spectroscopy
- Fourier transform nmr spectroscopy
- 11. Electron spin resonance spectrometers
- Electron spin resonance
- Basic esr spectrometer
- Detailed description of an esr spectrometer
- 12. Electron and ion spectrometers
- Surface spectroscopic techniques
- Electron spectroscopy
- Instrumentation for electron spectroscopy
- Ion spectroscopy
- Scanning tunnelling microscopy
- Atomic force microscopy.
- 13. Radiochemical instruments
- Fundamentals of radiochemical methods
- Radiation detectors
- Liquid scintillation counters
- Pulse?height analyzer
- Gamma spectrometry
- 14. X-ray spectrometers
- X-ray spectrum
- Instrumentation for x-ray spectrometry
- X-ray diffractometers
- X-ray absorption meter
- X-ray fluorescence spectrometry
- Electron probe microanalyzer
- 15. Automated chemical analysis systems
- Why automate?
- Automated biochemical analysis system
- Advanced versions of multiple analysis system
- Flow injection analysis (fia) technique
- Lab-on-chip technology for automated analysis
- 16. Gas chromatographs
- Chromatography
- Basic definitions
- Gas chromatography
- Basic parts of a gas chromatograph
- Methods of measurement of peak areas
- 17. Liquid chromatographs
- Liquid chromatography
- Types of liquid chromatography
- High pressure liquid chromatograph (hplc)
- Amino-acid analyzers
- 18. Thermo-analytical instruments
- Thermo-analytical methods
- Thermogravimetric analysis (tga)
- Differential thermal analysis (dta)
- Differential scanning calorimetry
- Simultaneous thermal analysis/mass spectrometer
- 19. Electrophoresis apparatus and densitometers
- Electrophoresis
- Electrophoresis techniques
- Paper electrophoresis
- Electrophoresis apparatus
- Spectrodensitometers
- Microprocessor-based densitometer
- Capillary electrophoresis
- Micro-electrophoresis
- Steps in the electrophoresis procedure requiring quality control
- Electrochemical cell
- Potentiostats
- Types of electrochemical methods
- Potentiometers
- Conductivity meters
- Voltametry
- Polarographs
- Coulometers
- Amperometers
- Aquameters
- Microcomputer-controlled electrochemical instrumentation
- 21. Ph meters and ion analyzers
- What is ph ?
- Principle of ph measurement
- Electrodes for ph measurement
- Ph meters
- Selective ion electrodes
- Ion analyzer
- Chemically sensitive semiconductor devices
- Biosensors
- 22. Blood gas analyzers
- Acid base balance
- Blood ph measurement
- Measurement of blood pco_2
- Blood po_2 measurement
- A complete blood gas analyzer
- 23. Industrial gas analyzers
- Types of gas analyzers
- Paramagnetic oxygen analyzer
- Magnetic wind instruments
- The electrochemical methods
- Infrared gas analyzers
- Thermal conductivity analyzers
- Analyzers based on gas density
- Method based on ionization of gases
- 24. Environmental pollution monitoring instruments
- Air pollution monitoring instruments
- Carbon monoxide
- Sulphur dioxide
- Nitrogen oxides
- Hydrocarbons
- Ozone
- Automated wet-chemical air analysis
- Water pollution monitoring instruments
- 25. Electronic devices and circuits
- Electronic components
- Passive components
- Semiconductor devices
- Transistors
- Integrated circuits
- Operational amplifiers
- Sources of noise in electronic circuits
- Sources of noise in low?level measurements
- Noise reduction techniques
- 26. Digital circuits
- Digital circuits
- Types of logic circuits
- Logic families
- Categories of ic's based on packing density
- Typical digital integrated circuits
- Semiconductor memories
- Microprocessor
- Microcontrollers
- Data converters
- Data acquisition systems for analytical instruments
- 27. Computer-based analytical instruments
- Computers in analytical laboratories
- Digital computer
- Microcomputers
- Components of a microcomputer
- Computer software
- Connecting laboratory instruments to computers
- A. References.